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020 _a1466593547
020 _a9781466593541
040 _cdlc
082 _a547.0078 LEO
100 _aJohn Leonard
_940753
222 _aacid added addition allow amount apparatus appropriate aqueous attached bath bubbler carefully carried Chapter chemical chemistry chromatography collect column common commonly compound connected containing cooling crystallization cylinder described distillation ensure equipment essential ether example experiment extraction Figure filter fitted flow fractions funnel give glass heat HPLC hydrogen important inert atmosphere inert gas involving laboratory liquid manifold material measured metal method needle normally Once organic particularly placed plate position possible prepared pressure procedure PTFE pump purification quantities range reaction flask reaction mixture reagents record references remove sample scale separate septum setup shown silica simple sodium solid solution solvent starting stirring sure syringe Table techniques temperature tion tube typically usually vacuum vacuum pump valve vent vessel volume work-up
245 _aAdvanced Practical Organic Chemistry
250 _a 3rd edition, illustrated
260 _aLondon
_bCRC Press
_c2013
300 _a 356 pages
505 _aContents: Chapter 1 General introduction Chapter 2 Safety Chapter 3 Keeping records of laboratory work Chapter 4 Equipping the laboratory and the bench Chapter 5 Purification and drying of solvents Preparation purification and handling Chapter 7 Gases Chapter 8 Vacuum pumps Chapter 9 Carrying out the reaction Chapter 10 Working up the reaction Chapter 11 Purification Chapter 12 Smallscale reactions Chapter 13 Largescale reactions Chapter 14 Special procedures Chapter 15 Characterization
520 _aAny research that uses new organic chemicals, or ones that are not commercially available, will at some time require the synthesis of such compounds. Therefore, organic synthesis is important in many areas of both applied and academic research, from chemistry to biology, biochemistry, and materials science. The third edition of a bestseller, Advanc
600 _xScience › Chemistry › General
_928638
600 _xMedical / Biochemistry
_926818
600 _xScience / Chemistry / General
_927800
600 _x Science / Chemistry / Industrial & Technical
_928328
600 _xScience / Chemistry / Organic
_927931
700 _aBarry Lygo
_940754
700 _a Garry Procter
_940755
942 _2ddc
_cEB
999 _c7863
_d7863